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Pdf analytical techniques for furosemide determination. The drug samples were used to prepare 100 mg l1 folic acid solutions, in triplicate. In this scientific work, it was developed a single analytical procedure for the sample preparation of different tissues of blue crabs using microwaveassisted digestion for the determination of cu, mn, fe and zn by fast sequential flame atomic absorption spectrometry fs faas. Skoog fundamentals of analytical chemistry 9th c2014 solutions ssm. The same procedure was used for the capsule form of the drug. Validation of analytical procedures using added samples as reference. These solutions were prepared in triplicate, and the accuracy was expressed in terms of the percentage recovery. Evaluation was made of intraday and interday precision. The validation of a test should include estimates of sensitivity, specificity and. Pdf critical evaluation of analytical procedures for the. Deter minationsthe sail method, y costas fotakis en relacion con las optical. Kealey university of surrey published by blackwell science ltd in 200 0 of professors of science faculties universities.
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